Development and Validation of Liquid Chromatography-Tandem Mass Spectrometry Method for Simultaneous Determination of Zinc Pyrithione and Pyrithione in Shampoos
DC Field | Value | Language |
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dc.contributor.author | Kim, T. H. | - |
dc.contributor.author | Jung, G. H. | - |
dc.contributor.author | Lee, E. H. | - |
dc.contributor.author | Park, H. R. | - |
dc.contributor.author | Lee, J. K. | - |
dc.contributor.author | Kim, H. G. | - |
dc.date.accessioned | 2021-08-11T11:44:00Z | - |
dc.date.available | 2021-08-11T11:44:00Z | - |
dc.date.issued | 2018-09 | - |
dc.identifier.issn | 1233-2356 | - |
dc.identifier.issn | 2083-5736 | - |
dc.identifier.uri | https://scholarworks.bwise.kr/sch/handle/2021.sw.sch/5700 | - |
dc.description.abstract | A simple, rapid, and sensitive liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed and validated for the determination of zinc pyrithione (ZnPT) and pyrithione (PT) in shampoos. The method consisted of a liquid-liquid extraction for sample preparation. The mass spectrometer was operated in multiple reaction monitoring (MRM) mode via the positive electrospray ionization interface. A linear regression (weighted 1/x) was used to fit calibration curves over the concentration range of 50-2000 ng/mL for both ZnPT and PT Excellent linearity (r(2) >= 0.9996) was achieved for all. The method was validated and found to be accurate (95.9-108.2% for ZnPT and 94.9-110.4% for PT), precise, and selective. Analytes in shampoos were found to be stable in the autosampler (6 degrees C for 6 h), in room temperature (for 6 h), and after three freeze-thaw cycles, and recovery of analytes was reproducible (90.8-94.6% for ZnPT and 90.2-96.3% for PT). | - |
dc.format.extent | 6 | - |
dc.language | 영어 | - |
dc.language.iso | ENG | - |
dc.publisher | Uniwersytet Slaski w Katowicach | - |
dc.title | Development and Validation of Liquid Chromatography-Tandem Mass Spectrometry Method for Simultaneous Determination of Zinc Pyrithione and Pyrithione in Shampoos | - |
dc.type | Article | - |
dc.publisher.location | 헝가리 | - |
dc.identifier.doi | 10.1556/1326.2017.00294 | - |
dc.identifier.scopusid | 2-s2.0-85049976668 | - |
dc.identifier.wosid | 000443278200011 | - |
dc.identifier.bibliographicCitation | Acta Chromatographica, v.30, no.3, pp 200 - 205 | - |
dc.citation.title | Acta Chromatographica | - |
dc.citation.volume | 30 | - |
dc.citation.number | 3 | - |
dc.citation.startPage | 200 | - |
dc.citation.endPage | 205 | - |
dc.type.docType | Article | - |
dc.description.isOpenAccess | N | - |
dc.description.journalRegisteredClass | scie | - |
dc.description.journalRegisteredClass | scopus | - |
dc.relation.journalResearchArea | Chemistry | - |
dc.relation.journalWebOfScienceCategory | Chemistry, Analytical | - |
dc.subject.keywordPlus | HAIR CARE PRODUCTS | - |
dc.subject.keywordPlus | ANTIFOULING COMPOUNDS | - |
dc.subject.keywordPlus | CARBON ELECTRODES | - |
dc.subject.keywordPlus | WATER SAMPLES | - |
dc.subject.keywordPlus | SEA-URCHIN | - |
dc.subject.keywordPlus | TOXICITY | - |
dc.subject.keywordPlus | COPPER | - |
dc.subject.keywordPlus | BIOCIDES | - |
dc.subject.keywordPlus | EMBRYOTOXICITY | - |
dc.subject.keywordPlus | PYRIDINETHIONE | - |
dc.subject.keywordAuthor | Pyrithione | - |
dc.subject.keywordAuthor | zinc pyrithione | - |
dc.subject.keywordAuthor | LC-MS/MS | - |
dc.subject.keywordAuthor | liquid-liquid extraction | - |
dc.subject.keywordAuthor | shampoos | - |
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