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A Facile Synthetic Method of Silver Nanoparticles with a Continuous Size Range from sub-10 nm to 40 nm

Authors
Piao, LonghaiLee, Kyung HoonMin, Byoung KounKim, WoongDo, Young RagYoon, Sungho
Issue Date
Jan-2011
Publisher
WILEY-V C H VERLAG GMBH
Keywords
Silver nanoparticle; Nanocrystalline materials; Decomposition
Citation
BULLETIN OF THE KOREAN CHEMICAL SOCIETY, v.32, no.1, pp 117 - 121
Pages
5
Journal Title
BULLETIN OF THE KOREAN CHEMICAL SOCIETY
Volume
32
Number
1
Start Page
117
End Page
121
URI
https://scholarworks.bwise.kr/cau/handle/2019.sw.cau/46433
ISSN
0253-2964
1229-5949
Abstract
Size-controlled Ag nanoparticles (NPs) were prepared from the decomposition of Ag(I) carboxylates using ethanolamine derivatives as a reducing agent without an additional stabilizing agent. The size of the Ag NPs with a narrow size distribution (sub-10 nm to ca. 40 nm) was controlled precisely by varying the processing parameters, such as the type of reducing agent and the chain length of the carboxylate in the Ag(I) carboxylate. The optical properties, surface composition and crystallinity of the Ag NPs were characterized by ultraviolet-visible spectroscopy, gas chromatography-mass spectrometry, thermal gravimetric analysis, transmission electron microscopy and X-ray diffraction.
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