Simultaneous quantitation of five flavonoid glycosides in Herba Epimedii by high-performance liquid chromatography-tandem mass spectrometry
DC Field | Value | Language |
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dc.contributor.author | Islam, Nurul M. | - |
dc.contributor.author | Yoo, Hye Hyun | - |
dc.contributor.author | Lee, Min Woo | - |
dc.contributor.author | Dong, Mi-Sook | - |
dc.contributor.author | Park, Young In | - |
dc.contributor.author | Jeong, Ha Sook | - |
dc.contributor.author | Kim, Dong-Hyun | - |
dc.date.accessioned | 2021-06-23T18:04:16Z | - |
dc.date.available | 2021-06-23T18:04:16Z | - |
dc.date.created | 2021-01-21 | - |
dc.date.issued | 2008-01 | - |
dc.identifier.issn | 0958-0344 | - |
dc.identifier.uri | https://scholarworks.bwise.kr/erica/handle/2021.sw.erica/42709 | - |
dc.description.abstract | A rapid and accurate reversed-phase liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) method has been developed and validated for the quantitative determination of five flavonoid glycosides, icariin, epimedin A, epimedin B, epimedin C and hyperin in Herba Epimedii. Chromatographic separations were performed using a C-18 narrow-bore HPLC column; a mixture of an aqueous solution of ammonium formate (pH 4.0) and acetonitrile was used as the mobile phase, with compounds detected in the positive ion mode with multiple-reaction monitoring using a triple-quadrupole mass spectrometer equipped with an electrospray ionisation interface. This method for the determination of the reported flavonoid glycosides was accurate and reproducible, with a lower limit of quantification of 0.5 mu g/mL. The standard calibration curves for the above-mentioned compounds were linear (r(2) > 0.998) over the concentration range 0.5-10.0 mu g/mL. The relative standard deviations for intra- and inter-day precision over the concentration range for the flavonoid glycosides were lower than 7.8% with accuracy between 90.1 and 111.0%. The established method was successfully applied to the quality assessment of samples of Herba Epimedii collected from Korea and China. Copyright (C) 2007 John Wiley & Sons, Ltd. | - |
dc.language | 영어 | - |
dc.language.iso | en | - |
dc.publisher | John Wiley & Sons Inc. | - |
dc.title | Simultaneous quantitation of five flavonoid glycosides in Herba Epimedii by high-performance liquid chromatography-tandem mass spectrometry | - |
dc.type | Article | - |
dc.contributor.affiliatedAuthor | Yoo, Hye Hyun | - |
dc.identifier.doi | 10.1002/pca.1018 | - |
dc.identifier.scopusid | 2-s2.0-39049132012 | - |
dc.identifier.wosid | 000253340200009 | - |
dc.identifier.bibliographicCitation | Phytochemical Analysis, v.19, no.1, pp.71 - 77 | - |
dc.relation.isPartOf | Phytochemical Analysis | - |
dc.citation.title | Phytochemical Analysis | - |
dc.citation.volume | 19 | - |
dc.citation.number | 1 | - |
dc.citation.startPage | 71 | - |
dc.citation.endPage | 77 | - |
dc.type.rims | ART | - |
dc.type.docType | Article | - |
dc.description.journalClass | 1 | - |
dc.description.isOpenAccess | N | - |
dc.description.journalRegisteredClass | scopus | - |
dc.relation.journalResearchArea | Biochemistry & Molecular Biology | - |
dc.relation.journalResearchArea | Plant Sciences | - |
dc.relation.journalResearchArea | Chemistry | - |
dc.relation.journalWebOfScienceCategory | Biochemical Research Methods | - |
dc.relation.journalWebOfScienceCategory | Plant Sciences | - |
dc.relation.journalWebOfScienceCategory | Chemistry, Analytical | - |
dc.subject.keywordPlus | CAPILLARY-ZONE-ELECTROPHORESIS | - |
dc.subject.keywordPlus | DIODE-ARRAY DETECTION | - |
dc.subject.keywordPlus | ICARIIN | - |
dc.subject.keywordPlus | CONSTITUENTS | - |
dc.subject.keywordPlus | EXTRACTS | - |
dc.subject.keywordPlus | KOREANUM | - |
dc.subject.keywordPlus | MS | - |
dc.subject.keywordAuthor | Herba Epimedii | - |
dc.subject.keywordAuthor | HPLC-MS/MS | - |
dc.subject.keywordAuthor | quantitative analysis | - |
dc.subject.keywordAuthor | flavonoid glycosides | - |
dc.identifier.url | https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/pca.1018 | - |
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