Fabrication of Vertically Aligned Ferroelectric Polyvinylidene Fluoride Mesoscale Rod Arrays
- Authors
- Kim, Dongjin; Hong, Seungbum; Hong, Jongin; Choi, Yoon-Young; Kim, Jiyoon; Park, Moonkyu; Sung, Tae-hyun; No, Kwangsoo
- Issue Date
- Dec-2013
- Publisher
- WILEY
- Keywords
- polyvinylidene (PVDF); piezoelectrics; mesoscale rods arrays; anodized alumina oxide (AAO)
- Citation
- JOURNAL OF APPLIED POLYMER SCIENCE, v.130, no.6, pp.3842 - 3848
- Indexed
- SCIE
SCOPUS
- Journal Title
- JOURNAL OF APPLIED POLYMER SCIENCE
- Volume
- 130
- Number
- 6
- Start Page
- 3842
- End Page
- 3848
- URI
- https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/161337
- DOI
- 10.1002/app.39415
- ISSN
- 0021-8995
- Abstract
- We have fabricated vertically aligned ferroelectric PVDF mesoscale rod arrays comprising and phases using a 200 nm diameter anodized aluminum oxide (AAO) as the porous template. We could synthesize the ferroelectric phase in mesoscale rod forms by combining the well-established recipe for crystallizing the phase using dimethyl sulfoxide (DMSO) at low temperature and template-guided infiltration processing for the rods using AAO. We measured the dimensions of the PVDF rods by scanning electron microscopy and identified the polymorph phases by X-ray diffraction and Fourier transform infrared spectroscopy. The length of the rods varied from 3.82 m to 1.09 m and the diameter from 232 nm to 287 nm when the volume ratio between DMSO and acetone changed from 5 : 5 to 10 : 0. We obtained well-defined piezoresponse hysteresis loops for all rods with remnant piezoresponse ranging from 2.12 pm/V to 5.04 pm/V and coercive voltage ranging from 2.29 V to 2.71 V using piezoresponse force microscopy. Our results serve as a processing platform for flexible electronic devices that need high capacitance and piezoelectric functionalities such as flexible memory devices or body energy harvesting devices for intelligent systems.
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