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액상환원공정을 이용한 백금 나노 입자의 합성Synthesis of Platinum Nanoparticles by Liquid Phase Reduction
- Other Titles
- Synthesis of Platinum Nanoparticles by Liquid Phase Reduction
- Issue Date
- Feb-2012
- Publisher
- 한국분말야금학회
- Keywords
- Polyol process; Platinum nano particle; Metal salt; Shape control
- Citation
- 한국분말야금학회지, v.19, no.1, pp 60 - 66
- Pages
- 7
- Indexed
- KCI
- Journal Title
- 한국분말야금학회지
- Volume
- 19
- Number
- 1
- Start Page
- 60
- End Page
- 66
- ISSN
- 1225-7591
2287-8173
- Abstract
- In this study, Platinum(Pt) nanoparticles were synthesized by using polyol process which is one of the liquid phase reduction methods. Dihydrogen hexachloroplatinate (IV) hexahydrate (H2PtCl6·6H2O), as a precursor, was dissolved in ethylene glycol and silver nitrate (AgNO3) was added as metal salt for shape control of Pt particle. Also,polyvinylpyrrolidone (PVP), as capping agent, was added to reduce the size of particle and to separate the particles. The size of Pt nanoparticles was evaluated particle size analyzer (PSA). The size and morphology of Pt nanoparticles were observed by transmission electron microscopy (TEM) and high resolution TEM (HRTEM). Synthesized Pt nanoparticles were studied with varying time and temperature of polyol process. Pt nanoparticles have been successfully synthesized with controlled sizes in the range 5-10 and 20-40 nm with cube and multiple-cube shapes.
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Collections - 서울 공과대학 > 서울 신소재공학부 > 1. Journal Articles
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