소결 공정 개선을 통한 미세 결정립 몰리브덴 소결체 제조Fabrication of Fine-grained Molybdenum Sintered Body via Modified Sintering Process
- Other Titles
- Fabrication of Fine-grained Molybdenum Sintered Body via Modified Sintering Process
- Authors
- Lee, Tae Ho; Kim, Se Hoon; Park, Min Suh; Suk, Myung-Jin; Kim, Young Do
- Issue Date
- Nov-2011
- Publisher
- KOREAN INST METALS MATERIALS
- Keywords
- nanostructured materials; powder processing; grain refinement; image analysis; two-step sintering
- Citation
- KOREAN JOURNAL OF METALS AND MATERIALS, v.49, no.11, pp.868 - 873
- Indexed
- SCIE
SCOPUS
KCI
- Journal Title
- KOREAN JOURNAL OF METALS AND MATERIALS
- Volume
- 49
- Number
- 11
- Start Page
- 868
- End Page
- 873
- URI
- https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/167296
- DOI
- 10.3365/KJMM.2011.49.11.868
- ISSN
- 1738-8228
- Abstract
- In this study, the fabrication of ultra fine grained Mo bulk was conducted. MoO(3) nanopowders were prepared by a high energy ball-milling process and then reduced at the temperature of 800 degrees C without holding time in H(2) atmosphere. The particle size of Mo nanopowder was similar to 150 nm and grain size was similar to 40 nm. The two-step process was employed for the sintering of Mo nanopowder to obtain fine grain size. The densification over 90% could be obtained by the two-step sintering with a grain size of less than 660 nm. For higher density, modified two-step sintering was designed. 95% of theoretical density with the grain size of 730 nm was obtained by the modified two-step sintering.
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