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Observation of mechanical fracture and corresponding domain structure changes of polycrystalline PbTiO3 nanotubes

Authors
Choi, HyunwooHong, SeungbumKim, YunseokKim, MyungjunSung, Tae-HyunShin, HyunjungNo, Kwangsoo
Issue Date
Feb-2011
Publisher
WILEY-V C H VERLAG GMBH
Keywords
ferroelectrics; nanotubes; domains; fracture; piezoresponse force microscopy
Citation
PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS, v.5, no.2, pp.59 - 61
Indexed
SCIE
SCOPUS
Journal Title
PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS
Volume
5
Number
2
Start Page
59
End Page
61
URI
https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/169084
DOI
10.1002/pssr.201004495
ISSN
1862-6254
Abstract
PbTiO3 (PTO) nanotubes (NTs) were synthesized at various temperatures by gas phase reaction between PbO gas and anatase TiO2 NTs and characterized by piezoresponse force microscopy (PFM). PTO ferroelectric phase was synthesized at as low as 400 degrees C as evidenced by PFM domain images and piezoresponse hysteresis loop measurement. Furthermore, the PTO NTs fabricated at above 500 degrees C underwent mechanical fracture through development of nanocracks due to grain growth, leading to ferroelectric domains with larger size and lower aspect ratio.
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