The Synthesis of a High Yield PbSe Quantum Dots by Hot Solution Methodopen access
- Authors
- Baek, In Chan; Seok, Sang Il; Chung, Yong-Chae
- Issue Date
- Sep-2008
- Publisher
- WILEY-V C H VERLAG GMBH
- Keywords
- PbSe; Quantum dots; Hot solution method
- Citation
- BULLETIN OF THE KOREAN CHEMICAL SOCIETY, v.29, no.9, pp.1729 - 1731
- Indexed
- SCIE
SCOPUS
KCI
- Journal Title
- BULLETIN OF THE KOREAN CHEMICAL SOCIETY
- Volume
- 29
- Number
- 9
- Start Page
- 1729
- End Page
- 1731
- URI
- https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/171894
- DOI
- 10.5012/bkcs.2008.29.9.1729
- ISSN
- 0253-2964
- Abstract
- Colloidal solutions of crystalline PbSe nanoparticles have been synthesized by hot Solution chemical process using PbO in oleic acid and tributylphosphine (TBP) bonded selenium. The use of TBP as a capping agent along with oleic acid gives a very good yield (around 10% at 180 degrees C) with an average diameter of particle of about < 6.6 nm. The effects of temperature on size and production yield of PbSe quantum dots are studied. X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM) and UV/VIS/NIR absorption spectroscopy were used to characterize the samples.
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