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The Synthesis of a High Yield PbSe Quantum Dots by Hot Solution Methodopen access

Authors
Baek, In ChanSeok, Sang IlChung, Yong-Chae
Issue Date
Sep-2008
Publisher
WILEY-V C H VERLAG GMBH
Keywords
PbSe; Quantum dots; Hot solution method
Citation
BULLETIN OF THE KOREAN CHEMICAL SOCIETY, v.29, no.9, pp.1729 - 1731
Indexed
SCIE
SCOPUS
KCI
Journal Title
BULLETIN OF THE KOREAN CHEMICAL SOCIETY
Volume
29
Number
9
Start Page
1729
End Page
1731
URI
https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/171894
DOI
10.5012/bkcs.2008.29.9.1729
ISSN
0253-2964
Abstract
Colloidal solutions of crystalline PbSe nanoparticles have been synthesized by hot Solution chemical process using PbO in oleic acid and tributylphosphine (TBP) bonded selenium. The use of TBP as a capping agent along with oleic acid gives a very good yield (around 10% at 180 degrees C) with an average diameter of particle of about < 6.6 nm. The effects of temperature on size and production yield of PbSe quantum dots are studied. X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM) and UV/VIS/NIR absorption spectroscopy were used to characterize the samples.
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