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Total Synthesis of (+/-)-Aspidospermidine Starting from 3-Ethyl-5-bromo-2-pyroneopen access
- Authors
- Cho, Hyun-Kyu; Tam, Nguyen Thanh; Cho, Cheon-Gyu
- Issue Date
- Nov-2010
- Publisher
- WILEY-V C H VERLAG GMBH
- Keywords
- Total synthesis; Aspidospermidine; Diels-Alder reaction; 3,5-Dibromo-2-pyrone; Tandem reaction
- Citation
- BULLETIN OF THE KOREAN CHEMICAL SOCIETY, v.31, no.11, pp.3382 - 3384
- Indexed
- SCIE
SCOPUS
KCI
- Journal Title
- BULLETIN OF THE KOREAN CHEMICAL SOCIETY
- Volume
- 31
- Number
- 11
- Start Page
- 3382
- End Page
- 3384
- ISSN
- 0253-2964
- Abstract
- A new synthetic route to (+/-)-aspidospermidine was devised, starting from the cycloadduct of 3-ethyl-5-bromo-2-pyrone with vinyl sulfide through a tandem conjugate addition-alkylation sequence The requisite 3-ethyl-5-bromo-2-pyrone was prepared via the C3-selective Pd-catalyzed coupling reaction with Et3Al-dimethylaminoethanol complex
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Related Researcher
- Cho, Cheon Gyu
- COLLEGE OF NATURAL SCIENCES (DEPARTMENT OF CHEMISTRY)