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초미세 결정립을 가지는 몰리브덴의 제조 및 기계적 특성Fabrication of Ultra Fine Grained Molybdenum and Mechanical Properties

Other Titles
Fabrication of Ultra Fine Grained Molybdenum and Mechanical Properties
Authors
김세훈서영익김대건석명진김영도
Issue Date
Jun-2010
Publisher
한국분말야금학회
Keywords
Nanostructured Mo powder; Two-step sintering; Spark plasma sintering; Ultra fine grained molybdenum
Citation
한국분말야금학회지, v.17, no.3, pp.235 - 241
Indexed
KCI
Journal Title
한국분말야금학회지
Volume
17
Number
3
Start Page
235
End Page
241
URI
https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/174551
DOI
10.4150/KPMI.2010.17.3.235
ISSN
1225-7591
Abstract
Mo nanopowder was synthesized by ball-milling and subsequent hydrogen-reduction of MoO3powder. To fabricate ultra fine grained molybdenum, two-step sintering and spark plasma sintering process were employed. The grain size of specimen by two-step sintering and spark plasma sintering was around 0.6μm and 0.4 μm, respectively. Mechanical properties of ultra fine grained Mo with relative density of above 90% were significantly improved at room and high temperatures comparing to commercial bulk Mo of 99%relative density. This result was mainly explained by the grain size refinement due to diffusion-controlled sintering.
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