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Preparation of silica-silver heterogeneous nanocomposite particles by one-pot preparation strategy using polyol process: Size-controlled immobilization of silver nanoparticles

Authors
Lee, Jong-MinKim, Dae-WookJun, Young-DooOh, Seong-Geun
Issue Date
Aug-2006
Publisher
PERGAMON-ELSEVIER SCIENCE LTD
Keywords
composite; metals; chemical synthesis; electron microscopy; optical properties
Citation
MATERIALS RESEARCH BULLETIN, v.41, no.8, pp.1407 - 1416
Indexed
SCIE
SCOPUS
Journal Title
MATERIALS RESEARCH BULLETIN
Volume
41
Number
8
Start Page
1407
End Page
1416
URI
https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/181169
DOI
10.1016/j.materresbull.2006.02.010
ISSN
0025-5408
Abstract
The size-controlled immobilization of silver nanoparticles onto the silica surface was carried out through one-pot process involving polyol process for the first time. Thiol groups were employed as a chemical protocol to make a binding bridge between silver nanoparticle and silica surface. The size of immobilized silver nanoparticles was controlled by reaction temperature and time at two different concentrations of silver nitrate: 1000 and 10,000 ppm. This one-pot process involving polyol process can simplify the conventional complex reaction process to control the size of immobilized metal nanoparticles. Also, this research can contribute to the immobilization of the other metals onto the inorganic supports and to the control of the size of immobilized metal particles.
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