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A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cellopen access

Authors
Husband, Rachel J.Strohm, CorneliusAppel, KarenBall, Orianna B.Briggs, RichardBuchen, JohannesCerantola, ValerioChariton, StellaColeman, Amy L.Cynn, HyunchaeDattelbaum, DanaDwivedi, AnandEggert, Jon H.Ehm, LarsEvans, William J.Glazyrin, KonstantinGoncharov, Alexander F.Graafsma, HeinzHoward, AlexHuston, LarissaHutchinson, Trevor M.Hwang, HuijeongJacob, SonyKaa, JohannesKim, JaeyongKim, MinseobKoemets, EgorKonôpková, ZuzanaLangenhorst, FalkoLaurus, TorstenLi, XinyangMainberger, JonaMarquardt, HaukeMcBride, Emma E.McGuire, ChristopherMcHardy, James D.McMahon, Malcolm I.McWilliams, R StewartMéndez, Alba S JMondal, AnshumanMorard, GuillaumeO'Bannon, Earl F.Otzen, ChristophPépin, Charles M.Prakapenka, Vitali B.Prescher, ClemensPreston, Thomas R.Redmer, RonaldRoeper, MichaelSanchez-Valle, CarmenSmith, DeanSmith, Raymond F.Sneed, DanielSpeziale, SergioSpitzbart, TobiasStern, StephanSturtevant, Blake T.Sztuk-Dambietz, JolantaTalkovski, PeterVelisavljevic, NenadVennari, CaraWu, ZhongyanYoo, Choong ShikZastrau, UlfJenei, ZsoltLiermann, Hanns Peter
Issue Date
Jul-2023
Publisher
INT UNION CRYSTALLOGRAPHY
Keywords
extreme conditions science; X-ray free-electron lasers; diamond anvil cells; dynamic compression
Citation
JOURNAL OF SYNCHROTRON RADIATION, v.30, pp.671 - 685
Indexed
SCIE
SCOPUS
Journal Title
JOURNAL OF SYNCHROTRON RADIATION
Volume
30
Start Page
671
End Page
685
URI
https://scholarworks.bwise.kr/hanyang/handle/2021.sw.hanyang/189669
DOI
10.1107/S1600577523003910
ISSN
0909-0495
Abstract
An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s-1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s-1 was observed during the fast compression of Au, while a strain rate of ∼1100 s-1 was achieved during the rapid compression of N2 at 23 TPa s-1. open access.
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