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"On-water" Photochemical Thiol-Ene Reaction of N-Enoxybenzotriazoles
- Authors
- Jung, Jong In; Lee, Jun Sup; Shin, Seunghoon
- Issue Date
- Oct-2025
- Publisher
- Georg Thieme Verlag
- Keywords
- On water; Photocatalysis; Thiol-ene reaction; Radical chain; Catalyst-free
- Citation
- Synthesis, v.57, no.20, pp 2963 - 2968
- Pages
- 6
- Indexed
- SCIE
SCOPUS
- Journal Title
- Synthesis
- Volume
- 57
- Number
- 20
- Start Page
- 2963
- End Page
- 2968
- ISSN
- 0039-7881
1437-210X
- Abstract
- We report herein a photochemical thiol-ene coupling using N-enoxybenzotriazoles, significantly accelerated under "on-water" conditions. This approach achieves efficient coupling within just five minutes via a remarkably rapid radical chain reaction, attributed to enhanced EDA formation and accelerated radical addition through a hydrophobic effect. The robustness of this method under various perturbation conditions underscores its potential for broad applications.
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Related Researcher
- Shin, Seung hoon
- COLLEGE OF NATURAL SCIENCES (DEPARTMENT OF CHEMISTRY)