Y2O3 첨가 탄소 프리폼에 Si 용융 침투에 의해 제조한 반응 소결 탄화규소RBSC Prepared by Si Melt Infiltration into the Y2O3 Added Carbon Preform
- Other Titles
- RBSC Prepared by Si Melt Infiltration into the Y2O3 Added Carbon Preform
- Authors
- 장민호; 조경식
- Issue Date
- Jan-2021
- Publisher
- 한국분말야금학회
- Keywords
- RBSC (reaction-bonded silicon carbide); Carbon preform; Liquid infiltration; Relative density
- Citation
- 한국분말야금학회지, v.28, no.1, pp 51 - 58
- Pages
- 8
- Journal Title
- 한국분말야금학회지
- Volume
- 28
- Number
- 1
- Start Page
- 51
- End Page
- 58
- URI
- https://scholarworks.bwise.kr/kumoh/handle/2020.sw.kumoh/25200
- ISSN
- 1225-7591
2287-8173
- Abstract
- The conversion of carbon preforms to dense SiC by liquid infiltration is a prospectively low-cost and reliable method of forming SiC-Si composites with complex shapes and high densities. Si powder was coated on top of a 2.0wt .% Y2O3-added carbon preform, and reaction bonded silicon carbide (RBSC) was prepared by infiltrating molten Si at 1,450oC for 1-8 h. Reactive sintering of the Y2O3-free carbon preform caused Si to be pushed to one side, thereby forming cracking defects. However, when prepared from the Y2O3-added carbon preform, a SiC-Si composite in which Si is homogeneously distributed in the SiC matrix without cracking can be produced. Using the Si + C → SiC reaction at 1,450oC, 3C and 6H SiC phases, crystalline Si, and Y2O3 were generated based on XRD analysis, without the appearance of graphite. The RBSC prepared from the Y2O3-added carbon preform was densified by increasing the density and decreasing the porosity as the holding time increased at 1,450oC. Dense RBSC, which was reaction sintered at 1,450oC for 4 h from the 2.0wt.% Y2O3-added carbon preform, had an apparent porosity of 0.11% and a relative density of 96.8%.
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