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Electrochemical oxidative bromolactonization of unsaturated carboxylic acids with sodium bromide: Synthesis of bromomethylated gamma-lactones
- Authors
- Kim, Rabin; Ha, Jeauk; Woo, Jiwon; Kim, Dae Young
- Issue Date
- 5-Jan-2022
- Publisher
- Elsevier BV
- Keywords
- Electrochemical reaction; Bromolactonization; y -Lactones; Anodic oxidation; Alkenoic acids
- Citation
- Tetrahedron Letters, v.88, no.0, pp 1 - 5
- Pages
- 5
- Journal Title
- Tetrahedron Letters
- Volume
- 88
- Number
- 0
- Start Page
- 1
- End Page
- 5
- ISSN
- 0040-4039
- Abstract
- Electrochemical oxidative bromination and cyclization sequences of unsaturated carboxylic acids were developed in this study. This approach is environmentally-friendly, using bromide anion as bromine radical precursor without external oxidizing reagents. The electrochemical protocol offers a facile way to prepare bromomethylated y-lactones derivatives in moderate to high yields. (c) 2021 Elsevier Ltd. All rights reserved.
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Related Researcher
- Kim, Dae Young
- College of Natural Sciences (Department of Chemistry)