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Photocatalytic reductive sulfonylation and 1,2-alkyl migration cascades of vinyl cyclobutanols: A synthesis of beta-sulfonated cyclopentanones
- Authors
- Kim, Joo Hee; Kim, Dae Young
- Issue Date
- 17-Jan-2020
- Publisher
- Marcel Dekker Inc.
- Keywords
- beta-sulfonated cyclopentanones; photoredox process; semipinacol-type rearrangement; sulfonyl chlorides; vinyl cyclobutanols
- Citation
- Synthetic Communications, v.50, no.2, pp 207 - 216
- Pages
- 10
- Journal Title
- Synthetic Communications
- Volume
- 50
- Number
- 2
- Start Page
- 207
- End Page
- 216
- ISSN
- 0039-7911
1532-2432
- Abstract
- A photoredox strategy to access beta-sulfonated cyclopentanones from the reaction of vinyl cyclobutanols with sulfonyl chlorides is described. This reaction employs the inexpensive and easily accessible sulfonyl chlorides as a sulfonyl radical source. The present synthetic protocol is a convenient way to prepare beta-sulfonated cyclopentanones.
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Related Researcher
- Kim, Dae Young
- College of Natural Sciences (Department of Chemistry)