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Synthesis of beta-Selenylated Cyclopentanones via Photoredox-Catalyzed Selenylation/Ring-Expansion Cascades of Alkenyl Cyclobutanols
- Authors
- Jung, Hye Im; Kim, Dae Young
- Issue Date
- Jul-2019
- Publisher
- Georg Thieme Verlag
- Keywords
- selenylation; semipinacol rearrangement; 1; 2-alkyl migration; 1-(1-arylvinyl)cyclobutanols; photoredox reaction
- Citation
- Synlett, v.30, no.11, pp 1361 - 1365
- Pages
- 5
- Journal Title
- Synlett
- Volume
- 30
- Number
- 11
- Start Page
- 1361
- End Page
- 1365
- ISSN
- 0936-5214
1437-2096
- Abstract
- A photoredox strategy to access beta-selenated cyclic ketone derivatives through the coupling reaction of 1-(1-arylvinyl)cyclobutanols with diselenides under blue LED irradiation and an air atmosphere was developed. This reaction employs the easily accessible and shelf-stable diselenides as a selenium radical source, and the reaction has advantages of mild reaction conditions and broad substrate scope.
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Related Researcher
- Kim, Dae Young
- College of Natural Sciences (Department of Chemistry)