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Fabrication and characterization nano porous anodic ZrO2 membranes by two-step anodizing

Authors
Seo, E.-Y.Choi, S.-K.Shin, I.-S.Kang, W.-K.
Issue Date
2013
Keywords
Anodizing; Electrochemistry; Nano-porous oxide film; ZrO2
Citation
Journal of the Korean Chemical Society, v.57, no.5, pp.547 - 553
Journal Title
Journal of the Korean Chemical Society
Volume
57
Number
5
Start Page
547
End Page
553
URI
http://scholarworks.bwise.kr/ssu/handle/2018.sw.ssu/12215
DOI
10.5012/jkcs.2013.57.5.547
ISSN
1017-2548
Abstract
Zirconium oxide (ZrO2) nano porous membranes were fabricated by electrochemical two-step anodization with an electropolished zirconium substrate in inorganic water-based and organic electrolyte systems containing small amounts of fluoride. Using two-step anodization and organic electrolytes, highly regular and ordered nanotubular ZrO2 oxide layers can be compared with aqueous electrolytes. The morphology and size of the nano porous layers were characterized by FE-SEM (field emission scanning electron microscopy), XRD (X-ray diffraction), and EDS (energy dispersive spectroscopy). Luminescence properties were investigated by photoluminescence measurements. Copyright © 2005 KCSNET.
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