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Synthesis of 2-Substituted Benzothiazoles by Visible Light-Driven Photoredox Catalysis
- Authors
- Yu, Chunghyeon; Lee, Kyungyub; You, Youngmin; Cho, Eun Jin
- Issue Date
- May-2013
- Publisher
- WILEY-V C H VERLAG GMBH
- Keywords
- benzothiazoles; benzothiazolines; CH oxidation; radical reaction; visible light
- Citation
- ADVANCED SYNTHESIS & CATALYSIS, v.355, no.8, pp 1471 - 1476
- Pages
- 6
- Journal Title
- ADVANCED SYNTHESIS & CATALYSIS
- Volume
- 355
- Number
- 8
- Start Page
- 1471
- End Page
- 1476
- ISSN
- 1615-4150
- Abstract
- An efficient method for synthesis of the widely applicable 2-substituted benzothiazoles has been developed. The process requires only 0.1mol% [Ru(bpy)3Cl2], O2, and visible light irradiation with substrates: 2-aminothiophenol and a variety of aldehydes. We established an oxidative quenching of the photoredox catalyst as being the key process in this photoelectrocatalytic cycle.
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