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Synthesis, solid-state structures and metal ion complexation behavior of 2-picolyloxy lariate ethers
- Authors
- Dalley, N. Kent; Olsher, Uriel; Lee, Jong Chan; Eley, Mark D.; Wang, Jing; Bartsch, Richard A.
- Issue Date
- Oct-2007
- Publisher
- Pergamon Press Ltd.
- Keywords
- Lariat ethers; Solid-state structures; Picrate extraction; Isothermal titration calorimetry
- Citation
- Tetrahedron, v.63, no.43, pp 10576 - 10580
- Pages
- 5
- Journal Title
- Tetrahedron
- Volume
- 63
- Number
- 43
- Start Page
- 10576
- End Page
- 10580
- ISSN
- 0040-4020
- Abstract
- Three new 2-picolyloxy lariat ether compounds are prepared and solid-state structures are determined for two of them. Complexation behavior for a series of lariat ethers with pyridyl-containing side arms toward alkali metal cations and Ag+ is assessed by two-phase metal picrate extraction from aqueous solutions into chloroform and in homogeneous solutions by isothermal titration calorimetry in methanol.
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