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Characteristics of Nano-Sized (Pb, La)TiO3 Powder Synthesized at Room Temperature

Authors
Rha, Sa-KyunLim, BoramiChoa, Yong-HoJeon, Min-SeokSong, Jun-KwangLee, Youn-Seoung
Issue Date
Feb-2012
Publisher
American Scientific Publishers
Keywords
(Pb, La)TiO3; High Energy Mechano-Chemical Technique; Milling Time; XPS; XAS
Citation
Journal of Nanoscience and Nanotechnology, v.12, no.2, pp.1192 - 1195
Indexed
SCIE
SCOPUS
Journal Title
Journal of Nanoscience and Nanotechnology
Volume
12
Number
2
Start Page
1192
End Page
1195
URI
https://scholarworks.bwise.kr/erica/handle/2021.sw.erica/33861
DOI
10.1166/jnn.2012.4614
ISSN
1533-4880
Abstract
We synthesized nano-sized (Pb, La)TiO3 powder using a high energy mechano-chemical technique at room temperature. By the results, nano-sized (Pb, La)TiO3 powder with perovskite structure was successfully synthesized from an oxide mixture using a high energy mechano-chemical technique without any post-annealing. The mechanically-synthesized (Pb, La)TiO3 powder consisted of nanometer sized particles and had very high homogeneity. According to increase of milling time, source phases such as Pb oxides and TiO2 disappeared and the perovskite PLT phase was formed by chemical reaction and the release of OH group.
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ERICA 공학대학 (DEPARTMENT OF MATERIALS SCIENCE AND CHEMICAL ENGINEERING)
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