PREPARATIVE ISOLATION AND PURIFICATION OF PRENYLATED ISOFLAVONOIDS FROM CUDRANIA TRICUSPIDATA FRUITS USING CENTRIFUGAL PARTITION CHROMATOGRAPHY
DC Field | Value | Language |
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dc.contributor.author | Jeon, Je-Seung | - |
dc.contributor.author | Kim, Sang-Min | - |
dc.contributor.author | Lee, Hee Ju | - |
dc.contributor.author | Um, Byung Hun | - |
dc.contributor.author | Kim, Hak Ki | - |
dc.contributor.author | Kim, Chul Young | - |
dc.date.accessioned | 2021-06-23T10:02:36Z | - |
dc.date.available | 2021-06-23T10:02:36Z | - |
dc.date.created | 2021-01-21 | - |
dc.date.issued | 2012-06 | - |
dc.identifier.issn | 1082-6076 | - |
dc.identifier.uri | https://scholarworks.bwise.kr/erica/handle/2021.sw.erica/36289 | - |
dc.description.abstract | Prenylated isoflavonoids such as 6,8-diprenylorobol, 6,8-diprenylgenistein and 4'-O-methylalpinumisoflavone were purified from n-hexane extract of C. tricuspidata fruits using centrifugal partition chromatography (CPC) with a n-hexane-ethyl acetate-methanol-water (7: 3: 6: 4, v/v, ascending mode) solvent system in a one-step within 200 min. One-step preparative CPC yielded 22.4 mg of 6,8-diprenylorobol and 26.7 mg of 6,8-diprenylgenistein with 95% and 85% purity, respectively, from 350 mg of crude hexane extract. Further purification by crystallization in methanol yielded 4'-O-methylalpinumisoflavone (9.3 mg) at over 95% purity based on the HPLC analysis. The chemical structures of purified compounds were elucidated by H-1, C-13 NMR, and ESI-MS. | - |
dc.language | 영어 | - |
dc.language.iso | en | - |
dc.publisher | TAYLOR & FRANCIS INC | - |
dc.title | PREPARATIVE ISOLATION AND PURIFICATION OF PRENYLATED ISOFLAVONOIDS FROM CUDRANIA TRICUSPIDATA FRUITS USING CENTRIFUGAL PARTITION CHROMATOGRAPHY | - |
dc.type | Article | - |
dc.contributor.affiliatedAuthor | Kim, Chul Young | - |
dc.identifier.doi | 10.1080/10826076.2011.621151 | - |
dc.identifier.scopusid | 2-s2.0-84862978577 | - |
dc.identifier.wosid | 000305566900011 | - |
dc.identifier.bibliographicCitation | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, v.35, no.11, pp.1607 - 1615 | - |
dc.relation.isPartOf | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES | - |
dc.citation.title | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES | - |
dc.citation.volume | 35 | - |
dc.citation.number | 11 | - |
dc.citation.startPage | 1607 | - |
dc.citation.endPage | 1615 | - |
dc.type.rims | ART | - |
dc.type.docType | Article | - |
dc.description.journalClass | 1 | - |
dc.description.isOpenAccess | N | - |
dc.description.journalRegisteredClass | scie | - |
dc.description.journalRegisteredClass | scopus | - |
dc.relation.journalResearchArea | Biochemistry & Molecular Biology | - |
dc.relation.journalResearchArea | Chemistry | - |
dc.relation.journalWebOfScienceCategory | Biochemical Research Methods | - |
dc.relation.journalWebOfScienceCategory | Chemistry, Analytical | - |
dc.subject.keywordPlus | XANTHONES | - |
dc.subject.keywordPlus | FLAVONOIDS | - |
dc.subject.keywordPlus | CONSTITUENTS | - |
dc.subject.keywordPlus | ANTIOXIDANT | - |
dc.subject.keywordPlus | SEPARATION | - |
dc.subject.keywordAuthor | 4 &apos | - |
dc.subject.keywordAuthor | -O-methylalpinumisoflavone | - |
dc.subject.keywordAuthor | 6,8-diprenylgenistein | - |
dc.subject.keywordAuthor | 6,8-diprenylorobol | - |
dc.subject.keywordAuthor | centrifugal partition chromatography | - |
dc.subject.keywordAuthor | Cudrania tricuspidata | - |
dc.subject.keywordAuthor | prenylated isoflavonoids | - |
dc.identifier.url | https://www.tandfonline.com/doi/full/10.1080/10826076.2011.621151 | - |
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