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Colloidal Palladium Nanoparticles with In Situ H2: Reducing System for alpha,beta-Unsaturated Carbonyl Compounds alpha alpha
- Authors
- De Castro, Kathlia A.; Oh, Seungchan; Yun, Jongchan; Lim, Jin Kyu; An, Gwangil; Kim, Dong Kook; Rhee, Hakjune
- Issue Date
- Sep-2009
- Publisher
- Marcel Dekker Inc.
- Keywords
- Hydride; hydrogenation; palladium nano-sized particle; saturated alcohol; -unsaturated carbonyl compounds
- Citation
- Synthetic Communications, v.39, no.19, pp 3509 - 3520
- Pages
- 12
- Indexed
- SCIE
SCOPUS
- Journal Title
- Synthetic Communications
- Volume
- 39
- Number
- 19
- Start Page
- 3509
- End Page
- 3520
- ISSN
- 0039-7911
1532-2432
- Abstract
- A new reducing system comprising Pd(OAc)2 and NaBH4 in methanol to generate palladium nanoparticles has been efficiently utilized to reduce a variety of unsaturated carbonyl compounds. These were reduced to their corresponding saturated alcohols and fully saturated compounds in selected cases. This protocol presents alternative and mild reaction conditions for reduction.
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Related Researcher
- Rhee, Hak june
- ERICA 공학대학 (ERICA 에너지바이오학과)