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Enantiomer separation of a novel aminothiazolecarboxamide fungicide using polysaccharide-derived chiral stationary phases
- Authors
- Kim, Byoung-Hyoun; Lee, Sang Uck
- Issue Date
- Nov-2005
- Publisher
- Preston Publications, Inc.
- Citation
- Journal of Chromatographic Science, v.43, no.10, pp 501 - 504
- Pages
- 4
- Indexed
- SCOPUS
- Journal Title
- Journal of Chromatographic Science
- Volume
- 43
- Number
- 10
- Start Page
- 501
- End Page
- 504
- ISSN
- 0021-9665
1945-239X
- Abstract
- The direct enantioseparation of a novel aminothiazolecarboxamide fungicide, ethaboxam, on polysaccharide-derived chiral stationary phases (CSPs) is described. Good resolution is achieved with several polysaccharide-derived CSPs. Chiralcel OD (OD-H) and Chiralpak AS are excellent for direct enantiomer separation of ethaboxam. The elution behavior and the effects of eluent composition on the resolution of ethaboxam are also investigated. Furthermore, the mechanism for chiral recognition using molecular mechanics is discussed.
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