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Electroplated NiCo Alloy with Low Residual Stress from the Sulfate Bath

Authors
Lee, Yong-SuLee, Jae-Ho
Issue Date
Apr-2020
Publisher
AMER SCIENTIFIC PUBLISHERS
Keywords
Electroplating; NiCo Alloy; Saccharin; Grain Refinement
Citation
SCIENCE OF ADVANCED MATERIALS, v.12, no.4, pp.609 - 612
Journal Title
SCIENCE OF ADVANCED MATERIALS
Volume
12
Number
4
Start Page
609
End Page
612
URI
https://scholarworks.bwise.kr/hongik/handle/2020.sw.hongik/12404
DOI
10.1166/sam.2020.3675
ISSN
1947-2935
Abstract
NiCo alloys are electroplated in sulfate bath. The concentration of cobalt sulfate and current density were varied to optimize the surface hardness. The properties of NiCo deposits were analyzed using field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The surface hardness of the NiCo alloy was increased up to 500 Hv at 24 wt% Co in the deposits due to the grain refinement. The size of grain was reduced to 12 nm. The residual stress of the deposits was varied from tensile to compressive as the saccharin concentration increased. The zero residual stress was achieved at 0.05 g/L saccharin addition.
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