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Synthesis and Characterizations of Surface-Coated Superparamagentic Magnetite Nanoparticles

Authors
Cha, Yu-JungKim, Min-JungChoa, Yong-HoKim, JongryoulNam, BaekilLee, JoonsikKim, Dong HoKim, Ki Hyeon
Issue Date
Feb-2010
Publisher
Institute of Electrical and Electronics Engineers
Keywords
Magnetic particle; magnetite; magnetization; polymer; superparamagnetic
Citation
IEEE Transactions on Magnetics, v.46, no.2, pp 443 - 446
Pages
4
Indexed
SCI
SCIE
SCOPUS
Journal Title
IEEE Transactions on Magnetics
Volume
46
Number
2
Start Page
443
End Page
446
URI
https://scholarworks.bwise.kr/erica/handle/2021.sw.erica/40017
DOI
10.1109/TMAG.2009.2033205
ISSN
0018-9464
1941-0069
Abstract
The uncoated magnetite and the 2, 3-meso-dimercaptosuccinic acid (DMSA)-coated Fe3O4 nanoparticles were synthesized by a co-precipitation method, respectively. The DMSA surface modification on magnetite nanoparticles was observed by FT-IR. The average particle sizes of the uncoated magnetite and the DMSA coated magnetite were exhibited approximately 10.4 and 12.3 nm by TEM results. DMSA surface-coated Fe3O4 can introduce a dense and thin outer hydroxyl group (-OH) shell. In order to characterize the magnetic behaviors, the magnetization processes of the magnetic nanoparticles were measured with the temperature range of 5 K to 300 K. The mean blocking temperatures of the uncoated Fe3O4 and the DMSA surface-coated Fe3O4 exhibited about 172 +/- 28 K and 215 +/- 30 K, respectively. The value of magnetization of the DMSA-coated Fe3O4 nanoparticles was not so different with that of the uncoated Fe3O4.
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Kim, Jong ryoul
ERICA 첨단융합대학 (ERICA 신소재·반도체공학전공)
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